4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

Base Information

Chemical Name:4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole
CAS No.:1408003-20-2
Molecular Formula:C₁₇H₁₉ClIN₃
Molecular Weight:427.715
Hs Code.:

Synonyms:4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

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Chemical Property of 4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

Chemical Property:

Purity/Quality:

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Technology Process of 4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

There total 9 articles about 4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1408003-10-0
{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

: 1408003-20-2
4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; for 2.5h;

Reference yield:

: 1257327-84-6
4-chloro-1-(cyclopropylmethyl)-5-methoxy-1H-benzotriazole

: 1408003-20-2
4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron tribromide / dichloromethane / 4 h / 0 - 20 °C

1.2: 0.5 h / pH > 10

1.3: pH 6 - 7

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

3.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1.5 h / 90 °C

4.1: lithium borohydride; methanol / dichloromethane / 4.5 h / 20 °C

4.2: 18 h

5.1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 2.5 h

With 1H-imidazole; methanol; potassium phosphate; lithium borohydride; iodine; boron tribromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 1408003-20-2
4-chloro-1-(cyclopropylmethyl)-5-[4-(iodomethyl)cyclohex-1-en-1-yl]-1H-benzotriazole

Guidance literature:: Multi-step reaction with 9 steps

1.1: acetic acid / dichloromethane / 1.08 h / 10 °C

1.2: 18 h / 10 - 20 °C

2.1: hydrogen / 3percent Pt/0.6percentVG/C, deGussa / ethanol / 2.5 h / 10 °C / 2068.65 Torr / Inert atmosphere

3.1: methanesulfonic acid; isopentyl nitrite / ethanol / 0.25 h

4.1: sulfuryl dichloride / acetic acid / 17 h / 0 - 20 °C

5.1: boron tribromide / dichloromethane / 4 h / 0 - 20 °C

5.2: 0.5 h / pH > 10

5.3: pH 6 - 7

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

7.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1.5 h / 90 °C

8.1: lithium borohydride; methanol / dichloromethane / 4.5 h / 20 °C

8.2: 18 h

9.1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 2.5 h

With 1H-imidazole; methanol; potassium phosphate; lithium borohydride; sulfuryl dichloride; methanesulfonic acid; hydrogen; iodine; boron tribromide; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; isopentyl nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; acetic acid;