{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

Base Information

Chemical Name:{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol
CAS No.:1408003-10-0
Molecular Formula:C₁₇H₂₀ClN₃O
Molecular Weight:317.818
Hs Code.:

Synonyms:{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

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Chemical Property of {4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

Chemical Property:

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Technology Process of {4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

There total 8 articles about {4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1408003-09-7
methyl 4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-ene-1-carboxylate

: 1408003-10-0
{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

Guidance literature:: methyl 4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-ene-1-carboxylate; With methanol; lithium borohydride; In dichloromethane; at 20 ℃; for 4.5h;

With water; sodium hydrogencarbonate; In dichloromethane; for 18h;

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 1408003-10-0
{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetic acid / dichloromethane / 1.08 h / 10 °C

1.2: 18 h / 10 - 20 °C

2.1: hydrogen / 3percent Pt/0.6percentVG/C, deGussa / ethanol / 2.5 h / 10 °C / 2068.65 Torr / Inert atmosphere

3.1: methanesulfonic acid; isopentyl nitrite / ethanol / 0.25 h

4.1: sulfuryl dichloride / acetic acid / 17 h / 0 - 20 °C

5.1: boron tribromide / dichloromethane / 4 h / 0 - 20 °C

5.2: 0.5 h / pH > 10

5.3: pH 6 - 7

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

7.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1.5 h / 90 °C

8.1: lithium borohydride; methanol / dichloromethane / 4.5 h / 20 °C

8.2: 18 h

With methanol; potassium phosphate; lithium borohydride; sulfuryl dichloride; methanesulfonic acid; hydrogen; boron tribromide; acetic acid; N-ethyl-N,N-diisopropylamine; isopentyl nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; dichloromethane; water; acetic acid;

Reference yield:

: 1257327-82-4
N₁-(cyclopropylmethyl)-4-methoxybenzene-1,2-diamine

: 1408003-10-0
{4-[4-chloro-1-(cyclopropylmethyl)-1H-benzotriazol-5-yl]cyclohex-3-en-1-yl}methanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanesulfonic acid; isopentyl nitrite / ethanol / 0.25 h

2.1: sulfuryl dichloride / acetic acid / 17 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 4 h / 0 - 20 °C

3.2: 0.5 h / pH > 10

3.3: pH 6 - 7

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

5.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1.5 h / 90 °C

6.1: lithium borohydride; methanol / dichloromethane / 4.5 h / 20 °C

6.2: 18 h

With methanol; potassium phosphate; lithium borohydride; sulfuryl dichloride; methanesulfonic acid; boron tribromide; N-ethyl-N,N-diisopropylamine; isopentyl nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; dichloromethane; water; acetic acid;