1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate

Base Information

• Chemical Name: 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate
• CAS No.: 1073183-65-9
• Molecular Formula: C₁₂H₁₃N₂O₂*F₆P
• Molecular Weight: 362.212
• Mol file: 1073183-65-9.mol

Synonyms:1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate

Chemical Property of 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate

There total 3 articles about 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-(3-formyl-4-hydroxybenzyl)-1-methyl-1H-imidazole-3-ium chloride (1073183-74-0) → 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate (1073183-65-9)

Guidance literature:

With hexafluorophosphoric acid; In water; at 20 ℃; for 4h; Cooling with ice;

Reference yield:

5-(chloromethyl)salicylaldehyde (23731-06-8) → 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate (1073183-65-9)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 3 h / 20 °C / Inert atmosphere

2: hexafluorophosphoric acid / water / 4 h / 20 °C / Cooling with ice

With hexafluorophosphoric acid; In water; toluene;

DOI:10.1139/v11-106

Reference yield:

salicylaldehyde (90-02-8) → 1-(3-formyl-4-hydroxybenzyl)-3-methylimidazolium hexafluorophosphate (1073183-65-9)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / water / 24 h / 20 °C

2: toluene / 3 h / 20 °C / Inert atmosphere

3: hexafluorophosphoric acid / water / 4 h / 20 °C / Cooling with ice

With hydrogenchloride; hexafluorophosphoric acid; In water; toluene;

DOI:10.1139/v11-106

upstream raw materials:

3-(3-formyl-4-hydroxybenzyl)-1-methyl-1H-imidazole-3-ium chloride

5-(chloromethyl)salicylaldehyde

salicylaldehyde

Downstream raw materials:

CH₃N₂C₃H₃CH₂C₆H₃(OH)CHNOH⁽¹⁺⁾*PF₆^(1-)=(CH₃NC₃H₃NCH₂C₆H₃(OH)CHNOH)PF₆