pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Base Information

Chemical Name:pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate
CAS No.:1173818-27-3
Molecular Formula:C₃₄H₄₇F₅O₁₄
Molecular Weight:774.731
Hs Code.:

Synonyms:pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

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Chemical Property of pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

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Technology Process of pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

There total 4 articles about pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)formic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 1173818-27-3
pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at -15 - 25 ℃; for 12h;
DOI:10.1007/s11426-010-4136-3

Reference yield:

: 852628-92-3
methyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)-ethoxy)benzoate

: 1173818-27-3
pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide monohydrate / methanol; water / 6 h / -5 - 25 °C

1.2: pH 5 - 6

2.1: dicyclohexyl-carbodiimide / dichloromethane / 12 h / -15 - 25 °C

With lithium hydroxide monohydrate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1007/s11426-010-4136-3

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1173818-27-3
pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 24 h

2: potassium carbonate / acetone / 24 h / Reflux; Inert atmosphere

3: water; lithium hydroxide / methanol / 12 h

4: dicyclohexyl-carbodiimide / diethylene glycol dimethyl ether / 0 - 20 °C

With water; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; lithium hydroxide; In methanol; dichloromethane; diethylene glycol dimethyl ether; acetone;