6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

Base Information

Chemical Name:6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol
CAS No.:1263383-01-2
Molecular Formula:C₃₉H₇₀N₂O₁₆
Molecular Weight:822.989
Hs Code.:

Synonyms:6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

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Chemical Property of 6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

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Technology Process of 6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

There total 3 articles about 6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1173818-27-3
pentafluorophenyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

: 359867-97-3
(S)-tert-butyl (5-amino-6-hydroxyhexyl)carbamate

: 1263383-01-2
6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -15 - 25 ℃;
DOI:10.1007/s11426-010-4136-3

Reference yield:

: (3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)formic acid

: 1263383-01-2
6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 12 h / -15 - 25 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / -15 - 25 °C

With N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1007/s11426-010-4136-3

Reference yield:

: 852628-92-3
methyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)-ethoxy)benzoate

: 1263383-01-2
6-(tert-butoxycarbonylamino)-2-(3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzamido)hexyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide monohydrate / methanol; water / 6 h / -5 - 25 °C

1.2: pH 5 - 6

2.1: dicyclohexyl-carbodiimide / dichloromethane / 12 h / -15 - 25 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -15 - 25 °C

With lithium hydroxide monohydrate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1007/s11426-010-4136-3