ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

Base Information

Chemical Name:ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate
CAS No.:128577-78-6
Molecular Formula:C₃₁H₃₄O₆S
Molecular Weight:534.673
Hs Code.:

Synonyms:ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

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Chemical Property of ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

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Technology Process of ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

There total 9 articles about ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 128577-78-6
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

Guidance literature:

Reference yield:

: 5851-37-6
4-(phenylthio)butan-1-ol

: 128577-78-6
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine (TEA) / diethyl ether

2: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

With sodium hydride; triethylamine; In diethyl ether;
DOI:10.1021/jm00172a020

Reference yield:

: 29193-72-4
ethyl 4-(phenylthio)butanoate

: 128577-78-6
ethyl 5-<3-(ethoxycarbonyl)benzoyl>-2-<4-(phenylthio)butoxy>benzenepropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 24 percent / LiAlH₄ / diethyl ether / 4 h / 25 °C

2: triethylamine (TEA) / diethyl ether

3: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

With lithium aluminium tetrahydride; sodium hydride; triethylamine; In diethyl ether;
DOI:10.1021/jm00172a020