tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

Base Information

Chemical Name:tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate
CAS No.:1229245-12-8
Molecular Formula:C₂₀H₂₇NO₄
Molecular Weight:345.439
Hs Code.:

Synonyms:tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

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Chemical Property of tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

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Technology Process of tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

There total 1 articles about tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229245-13-9
tert-butyl (3-bromo-5-formylbenzyl)cyclopropylcarbamate

: 165059-42-7,934342-48-0
(E)-3-methoxy-1-propenylboronic acid pinacol ester

: 1229245-12-8
tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

Guidance literature:: With sodium carbonate; trans-dichlorobis(triphenylphosphine)palladium(II); In water; N,N-dimethyl-formamide; at 90 ℃; for 6h; Inert atmosphere of nitrogen;

Reference yield:

: 1229245-12-8
tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

: 1229245-11-7
tert-butyl cyclopropyl[3-(3-methoxypropyl)-5-methylbenzyl]carbamate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃; for 3h;

Reference yield:

: 1229245-12-8
tert-butyl cyclopropyl{3-formyl-5-[(1E)-3-methoxy-1-propen-1-yl]benzyl}carbamate

: 1194488-58-8
N-[3-(3-methoxypropyl)-5-methylbenzyl]cyclopropanamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

2: hydrogenchloride / 1,4-dioxane; dichloromethane / 2 h / 20 °C

With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; ethyl acetate;