Technology Process of C17H19FO4S
There total 3 articles about C17H19FO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium fluoride;
In
acetone;
for 2h;
Inert atmosphere;
Reflux;
DOI:10.1021/jm301205j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; 18-crown-6 ether / acetone / 3 h / Reflux; Inert atmosphere
2.1: sodium sulfite / tetrahydrofuran; ethanol; water / 0.25 h / 160 °C / Microwave irradiation
2.2: 3 h / 50 °C / Inert atmosphere
3.1: ammonium fluoride / acetone / 2 h / Inert atmosphere; Reflux
With
ammonium fluoride; 18-crown-6 ether; potassium carbonate; sodium sulfite;
In
tetrahydrofuran; ethanol; water; acetone;
DOI:10.1021/jm301205j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium sulfite / tetrahydrofuran; ethanol; water / 0.25 h / 160 °C / Microwave irradiation
1.2: 3 h / 50 °C / Inert atmosphere
2.1: ammonium fluoride / acetone / 2 h / Inert atmosphere; Reflux
With
ammonium fluoride; sodium sulfite;
In
tetrahydrofuran; ethanol; water; acetone;
DOI:10.1021/jm301205j