C

Base Information

Chemical Name:C
CAS No.:1352234-75-3
Molecular Formula:C₂₇H₂₈N₂O₇S
Molecular Weight:524.595
Hs Code.:

Synonyms:C

Suppliers and Price of C

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C

Chemical Property:

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Technology Process of C

There total 20 articles about C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1453105-13-9
1-((2R,3R,3aS,7R,7aS)-7-(benzyloxy)-3,3a-dihydroxyoctahydrobenzofuran-2-yl)-5-methylpyrimidine-2,4(1H,3H)-dione

: 1005-56-7
phenylcarbonochloridothioate

: 1352234-75-3
C

Guidance literature:: With pyridine; In dichloromethane; at -20 - 20 ℃; for 6h;
DOI:10.1021/jo401166q

Reference yield:

: 1352234-70-8
1,2-O-isopropylidene-5-O-benzyl-6-deoxy-3,6-C-divinyl-α-D-gulofuranose

: 1352234-75-3
C

Guidance literature:: Multi-step reaction with 5 steps

1.1: dowex 50W₈X / 1,4-dioxane; water / 50 °C

1.2: 0 - 25 °C

2.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0 - 83 °C

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Reflux

4.1: hydrogen / palladium 10% on activated carbon / methanol

5.1: potassium carbonate; methanol

With methanol; N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; hydrogen; potassium carbonate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 1352234-73-1
C₂₂H₂₄N₂O₇

: 1352234-75-3
C

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol

2: potassium carbonate; methanol

With methanol; hydrogen; potassium carbonate; palladium 10% on activated carbon; In methanol;