2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide

Base Information

• Chemical Name: 2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide
• CAS No.: 126523-14-6
• Molecular Formula: C₂₄H₂₄BrNO₅
• Molecular Weight: 486.362

Synonyms:2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide

Chemical Property of 2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide

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Technology Process of 2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide

There total 2 articles about 2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-4-benzyloxy-5-methoxyphenylacetic acid (64434-31-7) → 2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide (126523-14-6)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl chloride

2: triethylamine

With oxalyl dichloride; triethylamine;

Reference yield:

4-benzyloxy-2-bromo-5-methoxyphenylacetic acid chloride (343232-31-5) + 3,4-dimethoxyaniline (6315-89-5) → 2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide (126523-14-6)

Guidance literature:

With triethylamine; Yield given;

Reference yield: 78.0%

2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-N-(3,4-dimethoxy-phenyl)-acetamide (126523-14-6) → [2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-ethyl]-(3,4-dimethoxy-phenyl)-amine (126523-15-7)

Guidance literature:

With aluminium hydride; In tetrahydrofuran;

upstream raw materials:

4-benzyloxy-2-bromo-5-methoxyphenylacetic acid chloride

3,4-dimethoxyaniline

2-bromo-4-benzyloxy-5-methoxyphenylacetic acid

Downstream raw materials:

[2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-ethyl]-(3,4-dimethoxy-phenyl)-amine

1-[2-(4-Hydroxy-3-methoxy-phenyl)-ethyl]-5,6-dimethoxy-1,3-dihydro-indol-2-one

2-benzyloxy-5,6,12,12a-tetrahydro-3,9,10-trimethoxydibenz[b,g]indolizine

1-[2-(4-Benzyloxy-2-bromo-5-methoxy-phenyl)-ethyl]-5,6-dimethoxy-1H-indole

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