1-(Methylnitrosoamino)-2-propanol

Base Information

Chemical Name:1-(Methylnitrosoamino)-2-propanol
CAS No.:1104874-94-3
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:
Mol file:1104874-94-3.mol

Synonyms:(S)-methyl 2-(hexanamido)-3-(4-hydroxyphenyl)propanoate

Suppliers and Price of 1-(Methylnitrosoamino)-2-propanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

DC Chemicals
Defensamide(MHP) >98%
100 mg
$ 450.00

DC Chemicals
Defensamide(MHP) >98%
250 mg
$ 750.00

ChemScene
MHP 98.02%
20mg
$ 720.00

ChemScene
MHP 98.02%
10mg
$ 408.00

ChemScene
MHP 98.02%
5mg
$ 240.00

ChemScene
MHP 98.02%
1mg
$ 120.00

Total 12 raw suppliers

Chemical Property of 1-(Methylnitrosoamino)-2-propanol

Chemical Property:

Boiling Point:490.9±35.0 °C(Predicted)
PKA:9.76±0.15(Predicted)
Density:1.117±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

Defensamide(MHP) >98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(Methylnitrosoamino)-2-propanol

There total 3 articles about 1-(Methylnitrosoamino)-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

: 3417-91-2
L-tyrosine methyl ester HCl

: 142-61-0
Hexanoyl chloride

: 1104874-94-3
(S)-methyl 2-(hexanamido)-3-(4-hydroxyphenyl)propanoate

Guidance literature:: L-tyrosine methyl ester HCl; With triethylamine; In dichloromethane;

Hexanoyl chloride; In dichloromethane; at 0 ℃;

Reference yield: 85.0%

: 1080-06-4
L-Tyr-OMe

: 142-62-1
hexanoic acid

: 1104874-94-3
(S)-methyl 2-(hexanamido)-3-(4-hydroxyphenyl)propanoate

Guidance literature:: hexanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 0.333333h; Cooling with ice;

L-Tyr-OMe; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1007/s12039-017-1298-y

Reference yield:

: 60-18-4,18875-48-4,25619-78-7,30704-25-7
L-tyrosine

: 1104874-94-3
(S)-methyl 2-(hexanamido)-3-(4-hydroxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 4 h / Reflux

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.33 h / Cooling with ice

2.2: 12 h / 20 °C

With sulfuric acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1007/s12039-017-1298-y