N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

Base Information

Chemical Name:N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide
CAS No.:176791-28-9
Molecular Formula:C₁₇H₂₂F₃N₃O₃S
Molecular Weight:405.441
Hs Code.:

Synonyms:N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

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Technology Process of N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

There total 12 articles about N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 176791-38-1
N-(2-Nitrophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

: 176791-28-9
N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

Guidance literature:: With copper acetylacetonate; sodium tetrahydroborate; In ethanol; for 1h;
DOI:10.1016/0040-4039(96)00306-1

Reference yield:

: 176791-35-8
N-<2-(2-Methylsulfonyloxyethyl)cyclohex-2-enyl>-N-(2-nitrophenyl)methanesulfonamide

: 176791-28-9
N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / NaN₃ / dimethylformamide / 4 h / 70 °C

2: NaBH₄, propane-1,3-dithiol, Et₃N / methanol / 48 h

3: Et₃N, 4-(dimethylamino)pyridine / tetrahydrofuran / 1.) 0 deg C to room temp., 24 h, 2.) room temp., 3 d

4: 70 percent / NaBH₄, Cu(acac)2 / ethanol / 1 h

With 1.3-propanedithiol; dmap; copper acetylacetonate; sodium tetrahydroborate; sodium azide; triethylamine; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 176649-80-2
N-<2-(2-Hydroxyethyl)cyclohex-2-enyl>-N-(2-nitrophenyl)methanesulfonamide

: 176791-28-9
N-(2-Aminophenyl)-N-<2-<2-(trifluoroacetamido)ethyl>cyclohex-2-enyl>methanesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 19 h / Ambient temperature

2: 96 percent / NaN₃ / dimethylformamide / 4 h / 70 °C

3: NaBH₄, propane-1,3-dithiol, Et₃N / methanol / 48 h

4: Et₃N, 4-(dimethylamino)pyridine / tetrahydrofuran / 1.) 0 deg C to room temp., 24 h, 2.) room temp., 3 d

5: 70 percent / NaBH₄, Cu(acac)2 / ethanol / 1 h

With 1.3-propanedithiol; dmap; copper acetylacetonate; sodium tetrahydroborate; sodium azide; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;