(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Base Information

Chemical Name:(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate
CAS No.:98736-90-4
Molecular Formula:C₂₅H₂₄N₂O₆
Molecular Weight:448.475
Hs Code.:

Synonyms:(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Suppliers and Price of (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

There total 3 articles about (+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 98736-89-1
C₃₂H₂₈N₂O₇

: 98736-90-4
(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Guidance literature:: With hydrogenchloride; In ethanol; for 24h; Heating;
DOI:10.1021/jm00151a013

Reference yield:

: 61849-27-2
(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4-(1H,3H)pyrimidinedione

: 98736-90-4
(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / 2-methyl-tetrahydro-furan / 70 h / 58 °C

2: 78 percent / aq. HCl / ethanol / 24 h / Heating

With pyridine; hydrogenchloride; In 2-methyltetrahydrofuran; ethanol;
DOI:10.1021/jm00151a013

Reference yield:

: 98-88-4
benzoyl chloride

: 98736-90-4
(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / 2-methyl-tetrahydro-furan / 70 h / 58 °C

2: 78 percent / aq. HCl / ethanol / 24 h / Heating

With pyridine; hydrogenchloride; In 2-methyltetrahydrofuran; ethanol;
DOI:10.1021/jm00151a013