C₂₄H₄₄O₅Si

Base Information

Chemical Name:C₂₄H₄₄O₅Si
CAS No.:944913-73-9
Molecular Formula:C₂₄H₄₄O₅Si
Molecular Weight:440.696
Hs Code.:

C<sub>24</sub>H<sub>44</sub>O<sub>5</sub>Si

Synonyms:C₂₄H₄₄O₅Si

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Chemical Property of C₂₄H₄₄O₅Si

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Technology Process of C₂₄H₄₄O₅Si

There total 10 articles about C₂₄H₄₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944913-68-2
C₂₅H₃₀O₃

: 944913-73-9
C₂₄H₄₄O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 70 percent / sodium; ammonia; tBuOH / diethyl ether / 0.05 h / -78 °C

2.1: imidazole / CH₂Cl₂ / 0.75 h / 22 °C

3.1: (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂ / benzene / 0.67 h / 22 °C

4.1: 1.034 g / hydrogen peroxide; KF; KHCO₃ / tetrahydrofuran; methanol; H₂O / 22 °C

5.1: 96 percent / 4-(dimethylamino)pyridine; triethylamine / CH₂Cl₂ / 4 h / 22 °C

6.1: 78 percent / CuCN / tetrahydrofuran / 22 h / -15 °C

7.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -78 °C

8.1: ozone; 2,6-lutidine / CH₂Cl₂; methanol / 0.17 h / -78 °C

8.2: 869 mg / sodium borohydride / CH₂Cl₂; methanol / 1 h / 22 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; potassium fluoride; ammonia; dihydrogen peroxide; sodium; potassium hydrogencarbonate; ozone; triethylamine; tert-butyl alcohol; (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; benzene;
DOI:10.1002/anie.200700501

Reference yield:

: 944913-67-1
C₁₇H₂₂O₃

: 944913-73-9
C₂₄H₄₄O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: NaI / silver(I) complex of chiral N-heterocyclic carbene; (2-iPrO-3-Ph-C₆H₃)CH=RuCl₂(PPh₃) / tetrahydrofuran / 20 h / -15 °C

2.1: 70 percent / sodium; ammonia; tBuOH / diethyl ether / 0.05 h / -78 °C

3.1: imidazole / CH₂Cl₂ / 0.75 h / 22 °C

4.1: (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂ / benzene / 0.67 h / 22 °C

5.1: 1.034 g / hydrogen peroxide; KF; KHCO₃ / tetrahydrofuran; methanol; H₂O / 22 °C

6.1: 96 percent / 4-(dimethylamino)pyridine; triethylamine / CH₂Cl₂ / 4 h / 22 °C

7.1: 78 percent / CuCN / tetrahydrofuran / 22 h / -15 °C

8.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -78 °C

9.1: ozone; 2,6-lutidine / CH₂Cl₂; methanol / 0.17 h / -78 °C

9.2: 869 mg / sodium borohydride / CH₂Cl₂; methanol / 1 h / 22 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; potassium fluoride; ammonia; dihydrogen peroxide; sodium; potassium hydrogencarbonate; ozone; triethylamine; sodium iodide; tert-butyl alcohol; silver(I) complex of chiral N-heterocyclic carbene; (2-iPrO-3-Ph-C₆H₃)CH=RuCl₂(PPh₃); (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; benzene;
DOI:10.1002/anie.200700501

Reference yield:

: 944913-69-3
C₂₅H₃₂O₃

: 944913-73-9
C₂₄H₄₄O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: imidazole / CH₂Cl₂ / 0.75 h / 22 °C

2.1: (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂ / benzene / 0.67 h / 22 °C

3.1: 1.034 g / hydrogen peroxide; KF; KHCO₃ / tetrahydrofuran; methanol; H₂O / 22 °C

4.1: 96 percent / 4-(dimethylamino)pyridine; triethylamine / CH₂Cl₂ / 4 h / 22 °C

5.1: 78 percent / CuCN / tetrahydrofuran / 22 h / -15 °C

6.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -78 °C

7.1: ozone; 2,6-lutidine / CH₂Cl₂; methanol / 0.17 h / -78 °C

7.2: 869 mg / sodium borohydride / CH₂Cl₂; methanol / 1 h / 22 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; ozone; triethylamine; (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂; In tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1002/anie.200700501