[(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4

Base Information

Chemical Name:[(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4
CAS No.:1322736-54-8
Molecular Formula:BF₄*C₄₇H₅₃N₂P₂Rh₂
Molecular Weight:1000.51
Hs Code.:

Synonyms:[(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4

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Chemical Property of [(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4

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Technology Process of [(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4

There total 1 articles about [(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 35138-22-8
bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

: 1322736-52-6
3,5-bis(diphenylphosphinoethyl)pyrazole

: 1322736-54-8
[(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4

Guidance literature:: With N(C₂H₅)3; In dichloromethane; under inert atmosphere; stirred for 2 min, added N(C2H5)3, stirred for 30 min; org. phase washed with deaerated water three times, dried over Na2SO4, filtered, evapd., residue crystd. from THF/ether;
DOI:10.1016/j.ica.2011.02.040

Reference yield: 97.0%

: 201230-82-2
carbon monoxide

: 1322736-54-8
[(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)(Rh(η2:η2-1,5-cyclooctadiene))2]BF4

: 1322736-58-2
[(μ-κ2:κ2-3,5-bis(diphenylphosphinoethyl)pyrazolato)Rh2(CO)2(μ-CO)]BF4

Guidance literature:: In tetrahydrofuran; under inert atmosphere; CO gas bubbled through suspn. of Rh compd. for 1h; volatiles removed under reduced pressure, residue crystd. from THF/ether;
DOI:10.1016/j.ica.2011.02.040