Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

Base Information

Chemical Name:Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester
CAS No.:133346-21-1
Molecular Formula:C₃₄H₄₅NO₅Si₂
Molecular Weight:603.906
Hs Code.:

Synonyms:Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

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Chemical Property of Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

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Technology Process of Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

There total 1 articles about Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32568-59-5
4-vinylphenyl benzoate

: 133346-20-0
2,4-di(t-butyldimethylsilyloxy)benzaldehyde oxime

: 133346-21-1
Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

Guidance literature:: With N-chloro-succinimide; water; potassium hydrogencarbonate; Yield given. Multistep reaction; 1.) AcOEt, 65 deg C, 0.5 h, 2.) 25 deg C, 24 h;

Reference yield: 64.0%

: 133346-21-1
Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

: 133346-23-3
5-(4-benzoyloxyphenyl)-3-(2,4-dihydroxyphenyl)isoxazoline

Guidance literature:: With potassium fluoride; sodium acetate; In acetic acid; for 2h; Heating;

Reference yield:

: 133346-21-1
Benzoic acid 4-{3-[2,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4,5-dihydro-isoxazol-5-yl}-phenyl ester

: 961-29-5,13745-20-5
isoliquirtigenin

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / sodium acetate, KF / acetic acid / 2 h / Heating

2: 75 percent / NaOH / methanol / 24 h

3: H₂, boric acid / Raney-Ni / methanol; H₂O / 1 h / Heating

4: aq. NaOH / 1 h / Heating

With potassium fluoride; sodium hydroxide; hydrogen; sodium acetate; boric acid; nickel; In methanol; water; acetic acid;