(R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

Base Information

Chemical Name:(R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione
CAS No.:1190929-88-4
Molecular Formula:C₁₇H₂₂O₅
Molecular Weight:306.359
Hs Code.:

Synonyms:(R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

Suppliers and Price of (R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

There total 2 articles about (R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1098073-50-7
5-(1-(4-methoxyphenyl)ethylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 557-20-0
diethylzinc

: 1190929-88-4
(R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: With C₄₄H₃₄NO₂P; copper(II) bis(trifluoromethanesulfonate); In 1,2-dimethoxyethane; hexane; at -40 - 20 ℃; optical yield given as %ee;
DOI:10.1021/ja9076815

Reference yield:

: 1186309-74-9
5-[1-(4-methoxyphenyl)propylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

: 544-97-8
dimethyl zinc(II)

: 1186309-84-1
(S)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1190929-88-4
(R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: dimethyl zinc(II); With C₄₄H₃₄NO₂P; copper (II) trifluoroacetate hydrate; In 1,2-dimethoxyethane; toluene; at -40 ℃; Inert atmosphere;

5-[1-(4-methoxyphenyl)propylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione; In 1,2-dimethoxyethane; toluene; at -40 - 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0029-1216845

Reference yield:

: 1190929-88-4
(R)-5-[2-(4-methoxyphenyl)butan-2-yl]-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1-methoxy-4-(1-(R)-methylpropyl)benzene

: (S)-2-(4-methoxyphenyl)butane

Guidance literature:: With methanol; palladium 10% on activated carbon; hydrogen; at 20 ℃; for 24h; under 760.051 Torr; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ja9076815