2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide

Base Information

• Chemical Name: 2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide
• CAS No.: 1297309-74-0
• Molecular Formula: C₁₃H₁₅N₅S
• Molecular Weight: 273.362

Synonyms:2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide

Chemical Property of 2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide

There total 1 articles about 2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

thiosemicarbazide (79-19-6) + methyl 5-methyl-2-phenyl-4-imidazolyl ketone (28824-91-1) → 2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide (1297309-74-0)

Guidance literature:

With hydrogenchloride; In ethanol; water; for 5h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

Reference yield: 68.0%

2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide (1297309-74-0) + 1-(N-phenylhydrazono)-1-chloropropanone (18440-58-9,1017827-91-6) → 4-methyl-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}-5-(2-phenylhydrazono)-2,5-dihydrothiazole (1297309-82-0)

Guidance literature:

With triethylamine; In ethanol; for 3h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

Reference yield: 66.0%

2-oxo-N-(4-chlorophenyl)propanehydrazonoyl chloride (18247-78-4,1338563-31-7) + 2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide (1297309-74-0) → 5-[2-(4-chlorophenyl)hydrazono]-4-methyl-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}-2,5-dihydrothiazole (1297309-84-2)

Guidance literature:

With triethylamine; In ethanol; for 3h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

upstream raw materials:

thiosemicarbazide

methyl 5-methyl-2-phenyl-4-imidazolyl ketone

Downstream raw materials:

2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}-2,9a-dihydrothiazolo[5,4-b]quinoxaline

5-(4-fluorobenzylidene)-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}-5-((1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)methylene)thiazolidin-4-one

5-{[3-(benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl]methylene}-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

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