methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Base Information

Chemical Name:methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate
CAS No.:1308255-68-6
Molecular Formula:C₁₅H₁₆BN₃O₆S
Molecular Weight:377.186
Hs Code.:

Synonyms:methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

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Chemical Property of methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

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Technology Process of methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

There total 4 articles about methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₅BF₃N₃O₇S

: 1308255-68-6
methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Guidance literature:: With ammonia; In methanol; at 100 ℃; for 2h; Sealed tube;

Reference yield:

: 6464-98-8
methyl 3-(aminophenyl)carbamate

: 1308255-68-6
methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

2: chlorosulfonic acid / 0 - 20 °C / Neat (no solvent)

3: 4-methyl-morpholine / 0.5 h / 20 °C

4: ammonia / methanol / 2 h / 100 °C / Sealed tube

With 4-methyl-morpholine; chlorosulfonic acid; ammonia; triethylamine; In methanol; dichloromethane;

Reference yield:

: 1308256-77-0
methyl 3-(2,2,2-trifluoroacetamido)phenylcarbamate

: 1308255-68-6
methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid / 0 - 20 °C / Neat (no solvent)

2: 4-methyl-morpholine / 0.5 h / 20 °C

3: ammonia / methanol / 2 h / 100 °C / Sealed tube

With 4-methyl-morpholine; chlorosulfonic acid; ammonia; In methanol;