(Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

Base Information

Chemical Name:(Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine
CAS No.:1284293-66-8
Molecular Formula:C₂₁H₂₅NO
Molecular Weight:307.436
Hs Code.:

Synonyms:(Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

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Chemical Property of (Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

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Technology Process of (Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

There total 3 articles about (Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 61699-43-2
methyl 1,1-pentamethyleneprop-2-ynyl carbonate

: 463930-74-7
N-benzyl-4-methyl-penta-2,3-dienamide

: 1284293-66-8
(Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

Guidance literature:: With trifuran-2-yl-phosphane; palladium diacetate; potassium carbonate; In dimethyl sulfoxide; at 38 ℃; for 14h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.01.041

Reference yield:

: 100-46-9
benzylamine

: 1284293-66-8
(Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 1.5 h / 20 °C / 19001.3 Torr / Autoclave

2: trifuran-2-yl-phosphane; palladium diacetate; potassium carbonate / dimethyl sulfoxide / 14 h / 38 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifuran-2-yl-phosphane; palladium diacetate; potassium carbonate; triethylamine; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/j.tet.2011.01.041

Reference yield:

: 6214-32-0
1-bromo-3-methylbuta-1,2-diene

: 1284293-66-8
(Z)-N-benzyl 4-(3',3'-pentamethylenepropa-1',2'-dienyl)-5,5-dimethylfuran-2(5H)-imine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 1.5 h / 20 °C / 19001.3 Torr / Autoclave

2: trifuran-2-yl-phosphane; palladium diacetate; potassium carbonate / dimethyl sulfoxide / 14 h / 38 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifuran-2-yl-phosphane; palladium diacetate; potassium carbonate; triethylamine; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/j.tet.2011.01.041