12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

Base Information

Chemical Name:12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole
CAS No.:934506-85-1
Molecular Formula:C₃₅H₃₁N₃
Molecular Weight:493.651
Hs Code.:

Synonyms:12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

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Chemical Property of 12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

Chemical Property:

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Technology Process of 12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

There total 7 articles about 12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (12-benzyl-11,12-dihydro-11,12-diaza-indeno[2,1-a]fluoren-5-ylmethyl)-(2,6-dimethyl-benzylidene)-amine

: 934506-85-1
12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jo062184r

Reference yield:

: 934506-84-0
12-benzyl-5-(aminomethyl)-11,12-dihydroindolo[2,3-a]carbazole

: 934506-85-1
12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: MS₄ Angstroem / tetrahydrofuran / 24 h / Heating

2: 448 mg / NaBH₄ / CH₂Cl₂; methanol / 2 h / 20 °C

With sodium tetrahydroborate; MS₄ Angstroem; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo062184r

Reference yield:

: 934506-81-7
12-benzyl-5-cyano-11,12-dihydroindolo[2,3-a]carbazole

: 934506-85-1
12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NaBH₄; CoCl₂*6H₂O / methanol; tetrahydrofuran / 1 h / 20 °C

2: MS₄ Angstroem / tetrahydrofuran / 24 h / Heating

3: 448 mg / NaBH₄ / CH₂Cl₂; methanol / 2 h / 20 °C

With sodium tetrahydroborate; MS₄ Angstroem; cobalt(II) chloride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo062184r