12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

Base Information

Chemical Name:12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone
CAS No.:934506-87-3
Molecular Formula:C₃₆H₂₉N₃O
Molecular Weight:519.646
Hs Code.:

Synonyms:12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

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Chemical Property of 12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

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Technology Process of 12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

There total 4 articles about 12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 934506-85-1
12-benzyl-5-[N-(2,6-dimethylbenzyl)aminomethyl]-11,12-dihydroindolo[2,3-a]carbazole

: 201230-82-2
carbon monoxide

: 934506-87-3
12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

Guidance literature:: With copper diacetate; air; palladium diacetate; In toluene; for 12h; under 760 Torr; Heating;
DOI:10.1021/jo062184r

Reference yield:

: 934506-81-7
12-benzyl-5-cyano-11,12-dihydroindolo[2,3-a]carbazole

: 934506-87-3
12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / NaBH₄; CoCl₂*6H₂O / methanol; tetrahydrofuran / 1 h / 20 °C

2: MS₄ Angstroem / tetrahydrofuran / 24 h / Heating

3: 448 mg / NaBH₄ / CH₂Cl₂; methanol / 2 h / 20 °C

4: 15 percent / Cu(OAc)2; air / Pd(OAc)2 / toluene / 12 h / 760 Torr / Heating

With sodium tetrahydroborate; copper diacetate; air; MS₄ Angstroem; cobalt(II) chloride; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo062184r

Reference yield:

: 934506-84-0
12-benzyl-5-(aminomethyl)-11,12-dihydroindolo[2,3-a]carbazole

: 934506-87-3
12-benzyl-6-(2,6-dimethylbenzyl)staurosporinone

Guidance literature:: Multi-step reaction with 3 steps

1: MS₄ Angstroem / tetrahydrofuran / 24 h / Heating

2: 448 mg / NaBH₄ / CH₂Cl₂; methanol / 2 h / 20 °C

3: 15 percent / Cu(OAc)2; air / Pd(OAc)2 / toluene / 12 h / 760 Torr / Heating

With sodium tetrahydroborate; copper diacetate; air; MS₄ Angstroem; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo062184r