L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

Base Information

Chemical Name:L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester
CAS No.:619337-66-5
Molecular Formula:C₁₈H₂₈NO₆P
Molecular Weight:385.397
Hs Code.:

Synonyms:L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

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Chemical Property of L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

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Technology Process of L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

There total 1 articles about L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.5%

: 1679-64-7
Monomethyl terephthalate

: 159171-46-7
diethyl (R)-(-)-(1-amino-3-methylbutyl)phosphonate

: 619337-66-5
L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; chlorotri(pyrrolidin-1-yl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1002/chem.200304783

Reference yield:

: 619337-66-5
L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

: N-(3-methyl-1-phosphono-butyl)-terephthalamic acid methyl ester

Guidance literature:: With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 19h;
DOI:10.1002/chem.200304783

Reference yield:

: 619337-66-5
L-N-[1-(diethoxyphosphoryl)-3-methylbutyl]terephthalamic acid methyl ester

: C₁₄H₁₈Cl₂NO₄P

Guidance literature:: Multi-step reaction with 2 steps

1: aq. Me₃SiBr / CH₂Cl₂ / 19 h / 20 °C

2: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 11 h

With oxalyl dichloride; trimethylsilyl bromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200304783