L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

Base Information

Chemical Name:L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester
CAS No.:619337-68-7
Molecular Formula:C₃₀H₃₆NO₆P
Molecular Weight:537.593
Hs Code.:

Synonyms:L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

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Chemical Property of L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

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Technology Process of L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

There total 5 articles about L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: C₁₄H₁₈Cl₂NO₄P

: 619337-68-7
L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at 20 ℃; for 13h;
DOI:10.1002/chem.200304783

Reference yield:

: 1679-64-7
Monomethyl terephthalate

: 619337-68-7
L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90.5 percent / chlorotripyrrolidinophosphonium hexafluorophosphate; N-methyl morpholine / CH₂Cl₂ / 48 h / 20 °C

2: aq. Me₃SiBr / CH₂Cl₂ / 19 h / 20 °C

3: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 11 h

4: N-methyl morpholine / CH₂Cl₂ / 13 h / 20 °C

With 4-methyl-morpholine; oxalyl dichloride; trimethylsilyl bromide; chlorotri(pyrrolidin-1-yl)phosphonium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200304783

Reference yield:

: 159171-46-7
diethyl (R)-(-)-(1-amino-3-methylbutyl)phosphonate

: 619337-68-7
L-N-{1-[bis-(3,5-dimethylphenoxy)phosphoryl]-3-methylbutyl}terephthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90.5 percent / chlorotripyrrolidinophosphonium hexafluorophosphate; N-methyl morpholine / CH₂Cl₂ / 48 h / 20 °C

2: aq. Me₃SiBr / CH₂Cl₂ / 19 h / 20 °C

3: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 11 h

4: N-methyl morpholine / CH₂Cl₂ / 13 h / 20 °C

With 4-methyl-morpholine; oxalyl dichloride; trimethylsilyl bromide; chlorotri(pyrrolidin-1-yl)phosphonium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200304783