N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

Base Information

Chemical Name:N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate
CAS No.:1270171-51-1
Molecular Formula:C₁₉H₂₈N₄O₅
Molecular Weight:392.455
Hs Code.:

Synonyms:N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

Chemical Property:

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Technology Process of N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

There total 4 articles about N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 3179-63-3
3-Dimethylamino-1-propanol

: 312921-96-3
4-[N-(3′-aminopropyl)-2-pyrrolidone]-3-nitrobenzenesulfonic acid

: 1270171-51-1
N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

Guidance literature:: With sulfuric acid or H₃PW₁₂O₄₀; In N,N-dimethyl-formamide; toluene; at 130 ℃; for 10h;
DOI:10.1007/s00726-010-0634-z

Reference yield:

: 7663-77-6
1-(3-aminopropyl)-2-pyrrolidone

: 1270171-51-1
N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 8 h / 85 °C

2: sulfuric acid or H₃PW₁₂O₄₀ / N,N-dimethyl-formamide; toluene / 10 h / 130 °C

With sulfuric acid or H₃PW₁₂O₄₀; In dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1007/s00726-010-0634-z

Reference yield:

: 96-99-1
4-chloro-3-nitrobenzoate

: 1270171-51-1
N,N-dimethylaminopropyl-4-[N-(3'-aminopropyl)-2-pyrrolidone]-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 8 h / 85 °C

2: sulfuric acid or H₃PW₁₂O₄₀ / N,N-dimethyl-formamide; toluene / 10 h / 130 °C

With sulfuric acid or H₃PW₁₂O₄₀; In dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1007/s00726-010-0634-z