C₂₂H₂₂FN₃O₄S

Base Information

Chemical Name:C₂₂H₂₂FN₃O₄S
CAS No.:1374233-66-5
Molecular Formula:C₂₂H₂₂FN₃O₄S
Molecular Weight:443.499
Hs Code.:

C<sub>22</sub>H<sub>22</sub>FN<sub>3</sub>O<sub>4</sub>S

Synonyms:C₂₂H₂₂FN₃O₄S

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Chemical Property of C₂₂H₂₂FN₃O₄S

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Technology Process of C₂₂H₂₂FN₃O₄S

There total 8 articles about C₂₂H₂₂FN₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1374233-65-4
C₂₃H₂₃F₄N₃O₇S₂

: 1374233-66-5
C₂₂H₂₂FN₃O₄S

Guidance literature:: With sodium acetate; (diphenylphosphin)ferrocene; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 3h; Inert atmosphere;

Reference yield:

: 31872-62-5
4-methoxy-3-nitro-pyridine

: 1374233-66-5
C₂₂H₂₂FN₃O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 24 h / 20 °C

2.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

3.1: dichloromethane / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

6.1: 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Reflux

6.2: 0 °C / pH 3 - 4

7.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 0.5 h / 0 °C

8.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 3 h / 80 °C / Inert atmosphere

With 2-(diethylamino)ethanethiol hydrochloride; hydrogen; sodium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; dmap; (diphenylphosphin)ferrocene; palladium 10% on activated carbon; palladium diacetate; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 33631-09-3
4-methoxypyridin-3-amine

: 1374233-66-5
C₂₂H₂₂FN₃O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2.1: dichloromethane / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

5.1: 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Reflux

5.2: 0 °C / pH 3 - 4

6.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 0.5 h / 0 °C

7.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 3 h / 80 °C / Inert atmosphere

With 2-(diethylamino)ethanethiol hydrochloride; sodium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In dichloromethane; N,N-dimethyl-formamide;