N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine
CAS No.:1101872-47-2
Molecular Formula:C₂₃H₃₁NO₅
Molecular Weight:401.503
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

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Chemical Property of N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

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Technology Process of N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

There total 2 articles about N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 939985-83-8
tert-butyl N-[2-(2-hydroxy-5-methoxyphenyl)ethyl]-carbamate

: 1101872-47-2
N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 20h;
DOI:10.1016/j.bmc.2008.10.048

Reference yield:

: 939985-83-8
tert-butyl N-[2-(2-hydroxy-5-methoxyphenyl)ethyl]-carbamate

: 1462-37-9
bromoethyl-2-benzyl ether

: 1101872-47-2
N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃;
DOI:10.1016/j.bmc.2010.05.025

Reference yield: 58.0%

: 1101872-47-2
N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine

: 149488-16-4
imidazole-1-carbothionic acid (5-bromopyridin-2-yl)amide

: 1101872-63-2
N-(5-bromo-2-pyridinyl)-N'-{2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethyl}thiourea

Guidance literature:: N-(tert-butoxycarbonyl)-2-[2-(2-benzyloxyethoxy)-5-methoxyphenyl]ethylamine; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.166667h;

imidazole-1-carbothionic acid (5-bromopyridin-2-yl)amide; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1016/j.bmc.2008.10.048