Technology Process of C39H41N3O6
There total 11 articles about C39H41N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide;
In
ethyl acetate; N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 48h;
DOI:10.1002/asia.201200617
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 6 h / Cooling with ice
2: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide; ethyl acetate / 48 h / 0 - 20 °C
3: sodium hydroxide / methanol / 10 h
4: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide; ethyl acetate / 48 h / 0 - 20 °C
With
thionyl chloride; dicyclohexyl-carbodiimide; sodium hydroxide;
In
methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/asia.201200617
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 7 h / 20 °C
2: triethylamine / dichloromethane / 16 h / 20 °C
3: tetrabutylammomium bromide; palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl acetamide / 15 h / 100 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 8 h / 20 °C
5: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide; ethyl acetate / 48 h / 0 - 20 °C
With
thionyl chloride; tetrabutylammomium bromide; palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; tris-(o-tolyl)phosphine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl acetamide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/asia.201200617