Technology Process of C42H50O6Si
There total 1 articles about C42H50O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: AcOH; H2SO4 / 0.83 h / 0 °C
2: 10.8 g / TMSOTf; activated molecular sieves 4 Angstroem / CH2Cl2; tetrahydrofuran / 1 h / 0 °C
With
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sulfuric acid; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol9902374
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
DOI:10.1021/ol9902374
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 5.0 g / TBAF; AcOH / tetrahydrofuran / 2 h / 20 °C
2: tetrahydrofuran; diethyl ether / 1 h / -78 - -20 °C
3: NaHCO3; Pb(OAc)4 / CH2Cl2 / 0.83 h
4: 2-methyl-2-butene; sodium chlorite; NaH2PO4 / 2-methyl-propan-2-ol; H2O / 20 °C
With
lead(IV) acetate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol9902374