(R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

Base Information

Chemical Name:(R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester
CAS No.:1424401-87-5
Molecular Formula:C₂₁H₂₅NO₇
Molecular Weight:403.432
Hs Code.:

Synonyms:(R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

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Chemical Property of (R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

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Technology Process of (R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

There total 5 articles about (R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1424401-85-3
(S)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester 1-tert-butyl ester

: 1424401-87-5
(R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm301346z

Reference yield:

: 1424401-79-5
6-((S)-4-benzyl-2-oxazolidine-3-yl)-6-hexanoic acid

: 1424401-87-5
(R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 64 h / 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / 20 °C

3.1: trifluoroacetic acid / tetrahydrofuran; dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hexamethyldisilazane; potassium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301346z

Reference yield:

: 1424401-81-9
6-((S)-4-benzyl-2-oxazolidine-3-yl)-6-hexanoic acid allyl ester

: 1424401-87-5
(R)-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanedioic acid 7-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / 20 °C

2.1: trifluoroacetic acid / tetrahydrofuran; dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hexamethyldisilazane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm301346z