5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

Base Information

Chemical Name:5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one
CAS No.:1567327-17-6
Molecular Formula:C₂₁H₂₄N₂O₃Se
Molecular Weight:431.393
Hs Code.:

Synonyms:5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

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Chemical Property of 5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

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Technology Process of 5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

There total 5 articles about 5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29608-05-7
1-(4-aminobenzyl)piperidine

: C₉H₈Cl₂O₃Se

: 1567327-17-6
5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 5.25h;
DOI:10.1016/j.bmc.2013.12.066

Reference yield:

: 5653-40-7
2-Amino-4,5-dimethoxybenzoic acid

: 1567327-17-6
5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; hydrogenchloride / water / 0.5 h / 0 °C

1.2: 2.5 h / 50 °C

2.1: thionyl chloride; N,N-dimethyl-formamide / 3 h / 85 °C

3.1: triethylamine / dichloromethane / 5.25 h / 0 - 20 °C

With hydrogenchloride; thionyl chloride; triethylamine; N,N-dimethyl-formamide; sodium nitrite; In dichloromethane; water;
DOI:10.1016/j.bmc.2013.12.066

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1567327-17-6
5,6-dimethoxy-2-(4-(piperidin-1-ylmethyl)phenyl)benzo[d][1,2]selenazol-3(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 3 h / 90 °C

2: 10% Pt/activated carbon; hydrogen / methanol / 6 h / 15514.9 Torr

3: triethylamine / dichloromethane / 5.25 h / 0 - 20 °C

With 10% Pt/activated carbon; hydrogen; potassium carbonate; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmc.2013.12.066