[(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

Base Information

Chemical Name:[(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile
CAS No.:211320-44-4
Molecular Formula:C₂₃H₁₉ClN₂O₂S
Molecular Weight:422.935
Hs Code.:

Synonyms:[(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

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Chemical Property of [(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

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Technology Process of [(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

There total 4 articles about [(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 14271-73-9
4-methylbenzoyl cyanide

: 211320-34-2
C₃₂H₂₇ClNO₂PS

: 211320-44-4
[(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

Guidance literature:: In toluene; for 20h; Heating;
DOI:10.1055/s-1998-2096

Reference yield:

: 107266-89-7
2-Amino-5-chlorobenzyl tolyl sulfone

: 211320-44-4
[(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, HCl, H₂O, 2.) NaN₃ / 1.) 0-5 deg C, 30 min, 2.) H₂O, r.t., 5 h

2: 93 percent / CH₂Cl₂ / 0 - 20 °C

3: 48 percent / toluene / 20 h / Heating

With hydrogenchloride; sodium azide; water; sodium nitrite; In dichloromethane; toluene;
DOI:10.1055/s-1998-2096

Reference yield:

: 107266-86-4
(5-Chloro-2-nitrophenyl)methyl 4-tolyl sulfone

: 211320-44-4
[(E)-4-Chloro-2-(toluene-4-sulfonylmethyl)-phenylimino]-p-tolyl-acetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: Sn, HCl, H₂O

2: 1.) NaNO₂, HCl, H₂O, 2.) NaN₃ / 1.) 0-5 deg C, 30 min, 2.) H₂O, r.t., 5 h

3: 93 percent / CH₂Cl₂ / 0 - 20 °C

4: 48 percent / toluene / 20 h / Heating

With hydrogenchloride; tin; sodium azide; water; sodium nitrite; In dichloromethane; toluene;
DOI:10.1055/s-1998-2096