2-Amino-5-chlorobenzyl tolyl sulfone

Base Information

• Chemical Name: 2-Amino-5-chlorobenzyl tolyl sulfone
• CAS No.: 107266-89-7
• Molecular Formula: C₁₄H₁₄ClNO₂S
• Molecular Weight: 295.79

Synonyms:2-Amino-5-chlorobenzyl tolyl sulfone

Chemical Property of 2-Amino-5-chlorobenzyl tolyl sulfone

Chemical Property:

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Technology Process of 2-Amino-5-chlorobenzyl tolyl sulfone

There total 1 articles about 2-Amino-5-chlorobenzyl tolyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(5-Chloro-2-nitrophenyl)methyl 4-tolyl sulfone (107266-86-4) → 2-Amino-5-chlorobenzyl tolyl sulfone (107266-89-7)

Guidance literature:

With hydrogenchloride; tin; In methanol; at 30 - 40 ℃;

DOI:10.1055/s-1986-33421

Reference yield: 97.0%

Trimethyl orthoacetate (1445-45-0) + 2-Amino-5-chlorobenzyl tolyl sulfone (107266-89-7) → N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester (107266-95-5)

Guidance literature:

With toluene-4-sulfonic acid; for 2h; Heating;

DOI:10.1055/s-1986-33421

Reference yield: 91.0%

2-Amino-5-chlorobenzyl tolyl sulfone (107266-89-7) + orthoformic acid triethyl ester (122-51-0) → N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-formimidic acid ethyl ester (107266-94-4)

Guidance literature:

With toluene-4-sulfonic acid; for 2h; Heating;

DOI:10.1055/s-1986-33421

upstream raw materials:

(5-Chloro-2-nitrophenyl)methyl 4-tolyl sulfone

Downstream raw materials:

N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

5-Chloro-2-(3,4-dimethoxy-phenyl)-1H-indole

[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-[1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-amine

N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-formimidic acid ethyl ester

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