(3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

Base Information

Chemical Name:(3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol
CAS No.:889662-81-1
Molecular Formula:C₂₅H₃₀O₅
Molecular Weight:410.51
Hs Code.:

Synonyms:(3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

There total 3 articles about (3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 889662-75-3
(S)-((3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-2,2-dimethylfuro[2,3-d][1,3]dioxol-5-yl)(4-methoxyphenyl)methanol

: 762-72-1
allyl-trimethyl-silane

: 889662-81-1
(3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

Guidance literature:: With zirconium(IV) chloride; In acetonitrile; at 20 ℃; for 0.833333h;
DOI:10.1021/jo052418r

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 889662-81-1
(3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 1 h / Heating

1.2: 88 percent / tetrahydrofuran / 4 h / 20 °C

2.1: 77 percent / ZrCl₄ / acetonitrile / 0.83 h / 20 °C

With zirconium(IV) chloride; magnesium; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo052418r

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 889662-81-1
(3aR,5R,6S,6aR)-6-(benzyloxy)-tetrahydro-5-((R)-1-(4-methoxyphenyl)but-3-enyl)-2,2-dimethyl-6-phenoxyfuro[3,2-d][1,3]dioxol

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 1 h / Heating

1.2: 88 percent / tetrahydrofuran / 4 h / 20 °C

2.1: 77 percent / ZrCl₄ / acetonitrile / 0.83 h / 20 °C

With zirconium(IV) chloride; magnesium; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo052418r