ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate

Base Information

• Chemical Name: ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate
• CAS No.: 84774-88-9
• Molecular Formula: C₂₀H₂₉NO₆
• Molecular Weight: 379.453

Synonyms:ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate

Chemical Property of ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate

Chemical Property:

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Technology Process of ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate

There total 1 articles about ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2,2-dimethyl-3-oxobutanoate (597-04-6) → ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate (84774-88-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Na / 1.) anhydrous Et₂O, 0-5 deg C, 2.) abs. ethanol, 0 deg C, 6h, 3.) RT, 4.) abs. ethanol, 1h

2: ethanol / 24 h / Ambient temperature

With sodium; In ethanol;

DOI:10.1021/jo00155a029

Reference yield: 58.0%

ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate (84774-88-9) → 3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)piperidine-2,4-dione (84752-42-1)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;

DOI:10.1021/jo00155a029

Reference yield: 33.0%

ethyl (Z)-2,2-dimethyl-3-oxo-5-<(3,4,5-trimethoxyphenethyl)amino>-4-pentenoate (84774-88-9) → 3,3-Dimethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-1H-pyridine-2,4-dione (84752-43-2)

Guidance literature:

With sodium ethanolate; In ethanol; for 0.5h; Heating;

DOI:10.1021/jo00155a029

upstream raw materials:

ethyl 2,2-dimethyl-3-oxobutanoate

Downstream raw materials:

3,3-Dimethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-1H-pyridine-2,4-dione

3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)piperidine-2,4-dione

4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

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