4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

Base Information

Chemical Name:4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone
CAS No.:84752-44-3
Molecular Formula:C₂₀H₂₉NO₆
Molecular Weight:379.453
Hs Code.:

Synonyms:4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

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Chemical Property of 4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

Chemical Property:

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Technology Process of 4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

There total 9 articles about 4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 84752-42-1
3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)piperidine-2,4-dione

: 107-21-1
ethylene glycol

: 84752-44-3
4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 24h; Heating;
DOI:10.1021/jo00155a029

Reference yield:

: 54-04-6
mescaline

: 84752-44-3
4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 24 h / Ambient temperature

2: 33 percent / sodium ethoxide / ethanol / 0.5 h / Heating

3: 90 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

4: 73 percent / p-TsOH / benzene / 24 h / Heating

With hydrogen; sodium ethanolate; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/jo00155a029

Reference yield:

: 597-04-6
ethyl 2,2-dimethyl-3-oxobutanoate

: 84752-44-3
4,4-(ethylenedioxy)-3,3-dimethyl-1-(3,4,5-trimethoxyphenethyl)-2-piperidinone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Na / 1.) anhydrous Et₂O, 0-5 deg C, 2.) abs. ethanol, 0 deg C, 6h, 3.) RT, 4.) abs. ethanol, 1h

2: ethanol / 24 h / Ambient temperature

3: 33 percent / sodium ethoxide / ethanol / 0.5 h / Heating

4: 90 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

5: 73 percent / p-TsOH / benzene / 24 h / Heating

With hydrogen; sodium ethanolate; sodium; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/jo00155a029