3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione

Base Information

• Chemical Name: 3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione
• CAS No.: 123351-47-3
• Molecular Formula: C₁₆H₁₄N₄S₂
• Molecular Weight: 326.446
• Mol file: 123351-47-3.mol

Synonyms:3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione

Chemical Property of 3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione

There total 2 articles about 3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

thiourea (17356-08-0) + benzil (134-81-6) → 3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione (123351-47-3)

Guidance literature:

With sodium hydroxide; In water; butan-1-ol; for 2.5h; Heating;

Reference yield: 30.0%

thiourea (17356-08-0) + benzil (134-81-6) → 5,5-diphenyl-2-thioxoimidazolidin-4-one (21083-47-6) + 3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione (123351-47-3)

Guidance literature:

With sodium hydroxide; In ethanol; water; for 2.5h; Heating;

Reference yield: 90.0%

3a,7a-diphenyltetrahydroimidazo<4,5-d>imidazole-2,5-dithione (123351-47-3) → 3a,6a-diphenylglycoluril (5157-15-3)

Guidance literature:

With tetrabromoglycoluril; In methanol; at 40 ℃; for 0.333333h; Reagent/catalyst; Green chemistry;

DOI:10.1134/S1070428019120108

upstream raw materials:

thiourea

benzil

Downstream raw materials:

3a,6a-diphenylglycoluril