C₄₄H₇₆O₉Si₃

Base Information

Chemical Name:C₄₄H₇₆O₉Si₃
CAS No.:153145-37-0
Molecular Formula:C₄₄H₇₆O₉Si₃
Molecular Weight:833.339
Hs Code.:

C<sub>44</sub>H<sub>76</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₄₄H₇₆O₉Si₃

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Chemical Property of C₄₄H₇₆O₉Si₃

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Technology Process of C₄₄H₇₆O₉Si₃

There total 10 articles about C₄₄H₇₆O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-16-1
methylmagnesium bromide

: 153145-36-9
C₄₃H₇₂O₉Si₃

: 153145-37-0
C₄₄H₇₆O₉Si₃

Guidance literature:: In dichloromethane; at -45 ℃; for 15h;

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-37-0
C₄₄H₇₆O₉Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-37-0
C₄₄H₇₆O₉Si₃

Guidance literature:: Multi-step reaction with 10 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

With potassium permanganate; potassium dihydrogenphosphate; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;