1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

Base Information

Chemical Name:1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene
CAS No.:1198164-15-6
Molecular Formula:C₂₁H₂₁BrF₆O₃
Molecular Weight:515.29
Hs Code.:

Synonyms:1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

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Chemical Property of 1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

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Technology Process of 1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

There total 4 articles about 1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1198164-16-7
(3-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)phenyl)methanol

: 1198164-15-6
1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 ℃;

Reference yield:

: 1198164-17-8
3-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)benzaldehyde

: 1198164-15-6
1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C

2: triphenylphosphine; carbon tetrabromide / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; carbon tetrabromide; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2016.05.048

Reference yield:

: 87199-16-4
3-Formylphenylboronic acid

: 1198164-15-6
1-(3-(bromomethyl)phenoxy)-4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: copper diacetate; pyridine / dichloromethane / 12 h / 20 °C / Molecular sieve

2: sodium tetrahydroborate / methanol / 1 h / 0 °C

3: triphenylphosphine; carbon tetrabromide / dichloromethane / 0 - 20 °C

With pyridine; sodium tetrahydroborate; carbon tetrabromide; copper diacetate; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2016.05.048