4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

Base Information

Chemical Name:4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene
CAS No.:74852-27-0
Molecular Formula:C₁₅H₂₀O₂S
Molecular Weight:264.389
Hs Code.:

Synonyms:4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

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Chemical Property of 4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

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Technology Process of 4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

There total 2 articles about 4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 60603-23-8
3-methoxy-1-methyl-4-phenylthiocyclohex-3-ene-1-carboxaldehyde

: 74852-27-0
4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.166667h;
DOI:10.1021/ja00530a041

Reference yield:

: 60603-16-9
2-methoxy-3-phenylthiobuta-1,3-diene

: 74852-27-0
4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-di-tert-butyl-4-methylphenol / neat (no solvent) / Heating

2: 93 percent / sodium borohydride / methanol / 0.17 h / 0 °C

With sodium tetrahydroborate; 2,6-di-tert-butyl-4-methyl-phenol; In methanol;
DOI:10.1021/ja00530a041

Reference yield:

: 74852-27-0
4-hydroxymethyl-2-methoxy-4-methyl-1-phenylthiocyclohexene

: 60603-32-9
2-acetoxy-5-benzoyloxymethyl-5-methylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1 h / 0 °C

2: 228 mg / aq. perchloric acid / acetonitrile / 4 h / 0 °C

3: 89 percent / benzene / 0.17 h / Heating

4: 86 percent / MCPBA / CH₂Cl₂ / 1.) -78 deg C, 30 min, 2.) room temperature, 16 h, reflux, 8 h

With pyridine; perchloric acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; benzene;
DOI:10.1021/ja00530a041