3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

Base Information

Chemical Name:3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide
CAS No.:188782-91-4
Molecular Formula:C₂₃H₃₃NO₃Si
Molecular Weight:399.605
Hs Code.:

Synonyms:3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

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Chemical Property of 3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

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Technology Process of 3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

There total 4 articles about 3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20921-02-2
7-methoxy-3,4-dihydro-2H-1-benzopyran-2-one

: 188782-91-4
3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) KOH / 1.) H₂O, EtOH, 2.) H₂O, EtOH, 150 min

2: 97 percent / imidazole / dimethylformamide / 116 h / 60 °C

3: oxalyl chloride / CH₂Cl₂; dimethylformamide / 0 deg C, 1,5 h; rt, 3 h

4: 4.14 g / diethyl ether; pyridine / 17 h / Ambient temperature

With 1H-imidazole; potassium hydroxide; oxalyl dichloride; In pyridine; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00007-0

Reference yield:

: 21144-17-2
3-(2'-hydroxy-4'-methoxyphenyl)propanoic acid

: 188782-91-4
3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / imidazole / dimethylformamide / 116 h / 60 °C

2: oxalyl chloride / CH₂Cl₂; dimethylformamide / 0 deg C, 1,5 h; rt, 3 h

3: 4.14 g / diethyl ether; pyridine / 17 h / Ambient temperature

With 1H-imidazole; oxalyl dichloride; In pyridine; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00007-0

Reference yield:

: 188782-89-0
t-butyldimethylsilyl 3-(2'-t-butyldimethylsilyloxy-4'-methoxyphenyl)propanoate

: 188782-91-4
3-[2-(tert-Butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-N-methyl-N-phenyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 0 deg C, 1,5 h; rt, 3 h

2: 4.14 g / diethyl ether; pyridine / 17 h / Ambient temperature

With oxalyl dichloride; In pyridine; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00007-0