diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Base Information

Chemical Name:diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate
CAS No.:1456602-26-8
Molecular Formula:C₃₇H₄₂NO₅P
Molecular Weight:611.718
Hs Code.:

Synonyms:diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Suppliers and Price of diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

There total 8 articles about diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1456602-22-4
diethyl 3-(4-phenoxybenzamido)benzylphosphonate

: 111818-33-8
1-(bromomethyl)-4-cyclohexylbenzene

: 1456602-26-8
diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Guidance literature:: diethyl 3-(4-phenoxybenzamido)benzylphosphonate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1h;

1-(bromomethyl)-4-cyclohexylbenzene; In tetrahydrofuran; mineral oil; at 20 ℃; for 16h;
DOI:10.1039/c3md20323a

Reference yield: 72.0%

: 1456602-26-8
diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1h;

In tetrahydrofuran; mineral oil; at 20 ℃; for 16h;

Reference yield:

: 92863-34-8
4-cyclohexylbenzoic acid methyl ester

: 1456602-26-8
diethyl 3-(N-(4-cyclohexylbenzyl)-4-phenoxybenzamido)benzylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

2.1: carbon tetrabromide / dichloromethane / 16 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

3.2: 16 h / 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c3md20323a