N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide

Base Information

• Chemical Name: N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide
• CAS No.: 155447-67-9
• Molecular Formula: C₁₈H₁₅F₃N₂O
• Molecular Weight: 332.325

Synonyms:N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide

Chemical Property of N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide

There total 3 articles about N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

N-(4-methoxyphenyl)-N'-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide → N1-(4-oxo-2,5-cyclohexadien-1-ylidene)-N2-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide (155447-67-9)

Guidance literature:

With water; In acetonitrile; at -10 ℃; electrolysis: NaClO₄, glassy carbon anode, platinum foil cathode; 5 mA/cm² for 2.5-3.0 F/mol;

DOI:10.1021/jo00090a017

Reference yield:

1-amino-5,6,7,8-tetrahydronaphthalene (2217-41-6) → N1-(4-oxo-2,5-cyclohexadien-1-ylidene)-N2-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide (155447-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / NaH / tetrahydrofuran / 0.5 h / 68 °C

2: 61 percent / H₂O / acetonitrile / -10 °C / electrolysis: NaClO₄, glassy carbon anode, platinum foil cathode; 5 mA/cm² for 2.5-3.0 F/mol

With water; sodium hydride; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo00090a017

Reference yield:

N-(4-methoxyphenyl)trifluoroacetimidoyl chloride (75999-66-5) → N1-(4-oxo-2,5-cyclohexadien-1-ylidene)-N2-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide (155447-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / NaH / tetrahydrofuran / 0.5 h / 68 °C

2: 61 percent / H₂O / acetonitrile / -10 °C / electrolysis: NaClO₄, glassy carbon anode, platinum foil cathode; 5 mA/cm² for 2.5-3.0 F/mol

With water; sodium hydride; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo00090a017

upstream raw materials:

1-amino-5,6,7,8-tetrahydronaphthalene

N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 155447-67-9 N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-(5,6,7,8-tetrahydro-1-naphthyl)-2,2,2-trifluoroethanimidamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send