2-phenyl>-3,4,4-trimethyloxazolinium iodide

Base Information

Chemical Name:2-phenyl>-3,4,4-trimethyloxazolinium iodide
CAS No.:84694-48-4
Molecular Formula:C₁₆H₂₆NOSi*I
Molecular Weight:403.379
Hs Code.:

2-<o-<(trimethylsilyl)methyl>phenyl>-3,4,4-trimethyloxazolinium iodide

Synonyms:2-phenyl>-3,4,4-trimethyloxazolinium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl>-3,4,4-trimethyloxazolinium iodide

Chemical Property:

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Technology Process of 2-phenyl>-3,4,4-trimethyloxazolinium iodide

There total 1 articles about 2-phenyl>-3,4,4-trimethyloxazolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84694-18-8
2-{o-[(trimethylsilyl)methyl]phenyl}-4,4-dimethyloxazoline

: 74-88-4
methyl iodide

: 84694-48-4
2-phenyl>-3,4,4-trimethyloxazolinium iodide

Guidance literature:: In acetonitrile; at 40 - 50 ℃; for 7h;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-48-4
2-phenyl>-3,4,4-trimethyloxazolinium iodide

: 84694-21-3
2-phenyl>-3,4,4-trimethyloxazolidine

Guidance literature:: With sodium tetrahydroborate; In methanol; at -78 ℃; for 0.0833333h; Yield given;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-48-4
2-phenyl>-3,4,4-trimethyloxazolinium iodide

: 84694-44-0
2--3,3,4(S)-trimethyl-5(R)-phenyloxazolidinium triflate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaBH₄, Et₃N, 2.) 5percent HCl / 1.) EtOH, -78 deg C, 1 min, 2.) -78 deg C -> RT, 3 h

3: 90 percent / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; triethylamine; In dichloromethane;
DOI:10.1021/ja00344a028