3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Base Information

Chemical Name:3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide
CAS No.:1258215-54-1
Molecular Formula:C₁₆H₁₉BrN₂O₃
Molecular Weight:367.242
Hs Code.:

Synonyms:3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

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Chemical Property of 3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

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Technology Process of 3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

There total 5 articles about 3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1291075-47-2
C₁₇H₂₀BrNO₃

: 1258215-54-1
3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Guidance literature:: With hydroxylamine potassium salt; In methanol; at 0 ℃;
DOI:10.1002/cmdc.201300393

Reference yield:

: 93633-32-0
5-methoxy-2-methylene-5-oxopentanoic acid

: 1258215-54-1
3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2: Grubbs catalyst first generation / dichloromethane

3: hydroxylamine potassium salt / methanol / 0 °C

With Grubbs catalyst first generation; dmap; hydroxylamine potassium salt; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.08.117

Reference yield:

: 1291072-99-5
C₁₉H₂₄BrNO₃

: 1258215-54-1
3-(1-(3-bromophenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs catalyst first generation / dichloromethane

2: hydroxylamine potassium salt / methanol / 0 °C

With Grubbs catalyst first generation; hydroxylamine potassium salt; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.08.117