Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

Base Information

Chemical Name:Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid
CAS No.:202271-46-3
Molecular Formula:C₃₂H₃₉ClO₇
Molecular Weight:571.11
Hs Code.:

Synonyms:Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

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Chemical Property of Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

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Technology Process of Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

There total 1 articles about Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 111-44-4
3-oxa-1,5-dichloropentane

: 202271-46-3
Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1055/s-1998-4480

Reference yield: 68.0%

: 112-60-7
Tetraethylene glycol

: 202271-46-3
Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

: 202271-48-5
2-{2-[2-(2-{2-[2-((2R,3R,4S,5R,6S)-4,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-ethanol

Guidance literature:: With potassium hydroxide; at 70 ℃; for 0.75h;
DOI:10.1055/s-1998-4480

Reference yield:

: 202271-46-3
Methyl-2,3,6-tri-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

: 2,3,6-Tri-O-benzoyl-1,4-O-(3,6,9,12,15-pentaoxaheptadecen-1,17-diyl)-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / KOH / 0.75 h / 70 °C

2: 94.5 percent / pyridine / 1 h / Ambient temperature

3: H₂ / Pd/C / ethyl acetate; ethanol / 12 h / Ambient temperature

4: pyridine / 1.5 h / Ambient temperature

5: 88 percent / AcCl, MeOH / 1.5 h / Ambient temperature

6: 25 percent / BF₃*Et₂O, KBF₄ / acetonitrile / 3 h / Ambient temperature

With pyridine; methanol; potassium hydroxide; boron trifluoride diethyl etherate; hydrogen; potassium tetrafluoroborate; acetyl chloride; palladium on activated charcoal; In ethanol; ethyl acetate; acetonitrile;
DOI:10.1055/s-1998-4480