4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Base Information

Chemical Name:4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane
CAS No.:1314032-93-3
Molecular Formula:C₂₅H₄₂N₄O₂
Molecular Weight:430.634
Hs Code.:

Synonyms:4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

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Chemical Property of 4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

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Technology Process of 4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

There total 3 articles about 4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2Br^(1-)*C₂₅H₄₀N₄O₂⁽²⁺⁾

: 1314032-93-3
4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 192h;
DOI:10.1039/c0dt01395a

Reference yield:

: 1314032-85-3
Br^(1-)*C₁₉H₂₉N₄⁽¹⁺⁾

: 1314032-93-3
4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 384 h

2: sodium tetrahydroborate / ethanol / 192 h / 20 °C

With sodium tetrahydroborate; In ethanol; acetonitrile;
DOI:10.1039/c0dt01395a

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1314032-93-3
4-benzyl-11-(tert-butylcarboxy)methyl-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 384 h

2: sodium tetrahydroborate / ethanol / 192 h / 20 °C

With sodium tetrahydroborate; In ethanol; acetonitrile;
DOI:10.1039/c0dt01395a