5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

Base Information

Chemical Name:5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione
CAS No.:120121-21-3
Molecular Formula:C₁₇H₁₄Cl₂N₂O₄S
Molecular Weight:413.281
Hs Code.:

Synonyms:5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

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Technology Process of 5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

There total 5 articles about 5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 120121-44-0
5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethylsulfanyl]-phenyl}-imidazolidine-2,4-dione

: 120121-21-3
5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

Guidance literature:: With potassium permanganate; acetic acid; In water; at 0 ℃; for 0.5h;
DOI:10.1021/jm00126a011

Reference yield:

: 20324-50-9
5-chloro-2-mercapto-benzoic acid

: 120121-21-3
5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 35.0 g / lithium aluminium hydride / tetrahydrofuran / 3 h / Ambient temperature

2: 1) sodium methoxide / 1) N,N-dimethylformamide, 0 deg C, 30 min, 2) 30 min

3: manganese dioxide / CH₂Cl₂ / 6 h / Ambient temperature

4: 52 percent / aq. ethanol / 24 h / 60 °C

5: 78 percent / potassium permanganate, glacial acetic acid / H₂O / 0.5 h / 0 °C

With manganese(IV) oxide; potassium permanganate; lithium aluminium tetrahydride; sodium methylate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00126a011

Reference yield:

: 120121-37-1
4-chloro-2-(hydroxymethyl)thiophenol

: 120121-21-3
5-{5-Chloro-2-[2-(4-chloro-phenyl)-ethanesulfonyl]-phenyl}-imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 1) sodium methoxide / 1) N,N-dimethylformamide, 0 deg C, 30 min, 2) 30 min

2: manganese dioxide / CH₂Cl₂ / 6 h / Ambient temperature

3: 52 percent / aq. ethanol / 24 h / 60 °C

4: 78 percent / potassium permanganate, glacial acetic acid / H₂O / 0.5 h / 0 °C

With manganese(IV) oxide; potassium permanganate; sodium methylate; acetic acid; In ethanol; dichloromethane; water;
DOI:10.1021/jm00126a011