n-calix[3]amide

Base Information

Chemical Name:n-calix[3]amide
CAS No.:1370017-12-1
Molecular Formula:C₆₃H₇₈N₆O₃
Molecular Weight:967.351
Hs Code.:

Synonyms:n-calix[3]amide

Suppliers and Price of n-calix[3]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-calix[3]amide

Chemical Property:

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Technology Process of n-calix[3]amide

There total 1 articles about n-calix[3]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 1370017-12-1
n-calix[3]amide

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / Inert atmosphere

2: tin(ll) chloride / tetrahydrofuran; ethanol / Reflux; Inert atmosphere

3: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / Reflux; Inert atmosphere

5: lithium hexamethyldisilazane / tetrahydrofuran / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; tin(ll) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; water; 4: Suzuki coupling;
DOI:10.1246/cl.2012.249

Reference yield:

: 137846-38-9
{(1,3-bis(diphenylphosphino)propane)ditriflatopalladium(II)}

: 1370017-12-1
n-calix[3]amide

: (n-calix[3]amide)2(Pd(dppp))3(OTf)6

Guidance literature:: In chloroform-d1; d⁽⁴⁾-methanol; ligand and Pd complex mixed in molar ratio 2:3 in CDCl3/CH3OD (5/1 v/v); not isolated, detcd. by NMR;
DOI:10.1246/cl.2012.249