11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline

Base Information

Chemical Name:11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline
CAS No.:1574324-05-2
Molecular Formula:C₂₅H₁₇F₃N₄O₂
Molecular Weight:462.431
Hs Code.:

Synonyms:11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline

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Chemical Property of 11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline

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Technology Process of 11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline

There total 2 articles about 11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1574324-33-6
5,6-dimethoxy-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-(phenylethynyl)-1H-indole

: 1574324-05-2
11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline

Guidance literature:: With sodium azide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 120 ℃; for 7h; Inert atmosphere;
DOI:10.1021/jo402783p

Reference yield:

: 367-86-2
1-fluoro-2-nitro-4-trifluoromethyl-benzene

: 1369424-86-1
5,6-dimethoxy-2-(2-phenylethynyl)-1H-indole

: 1574324-05-2
11,12-dimethoxy-1-phenyl-6-(trifluoromethyl)indolo[1,2-a][1,2,3]triazolo[5,1-c]quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N,N,N,N,N-hexamethylphosphoric triamide / 7 h / 120 °C / Inert atmosphere

With sodium azide; sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide;
DOI:10.1021/jo402783p